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To a cooled (ice-bath) mixture of the obtained HCl salt in DMF (2 mL) were subsequently added a solution of XX21 (0.39 M in DMF, 0.292 mL, 0.113 mmol), HATU (51.4 mg, 0.135 mmol) and DIPEA (0.118 mL, 0.675 mmol) and the resulting mixture was stirred for 15 min at 4° C